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Facilities and Equipment

The laboratory is located in Piraeus, in privately owned facilities, in a building complex of 600 m2 , near the central port.

We have centralized all our services in one site in order to facilitate the teamwork and the cooperation between laboratories. The building is designed specifically for laboratory use and includes, besides the laboratories and the administrative offices, special spaces for storage of samples in controlled conditions.

In Tsakalidis Analysis&Testing we operate the following sections :

Chromatography laboratory
Spectroscopy laboratory
Wet Chemistry laboratory
Microbiological laboratory
Organoleptic Test laboratory

 
 
The CHROMATOGRAPHY LABORATORY  uses instruments of gas and liquid chromatography equipped with a  series of selective detectors  and detectors of general use.

For the identification and the even more sensitive quantitification needed for some demanding applications, the laboratory has  mass spectrometers of simple and triple quadrupole both in gas and liquid chromatography
                                                                                                                  
Aiming to the increase of productivity of our laboratory, all of our instruments are fitted with automatic samplers which allow the overnight operation and they are connected to a central system LIMS. For the preparation of the samples we use SPE, SPME techniques, liquid-liquid extraction and head space for the volatile compounds.

Some of our basic instruments are:

Gas chromatography systems with : 
mass spectrometer quadrupole detector (GC-MS) 
flame ionisation detector (FID)
electron capture detector (ECD)  
nitrogen-phosphorous detector (NPD
flame photometric detector(FPD)
 
Liquid chromatography systems with:  

mass spectrometer tandem quadrupole detector (LC-MS/MS)
fluorence detector with post-column derivatization
diode array detector (Diode Array)
ultraviolet-visible detector(UV-VIS)
refractive index detector(R.I.)
ion chromatography (I.C.)
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The SPECTROSCOPY LABORATORY has the required equipment for the determination of most of the metal in all kinds of substrates (solid, aqueous and organic) using the technique of atomic absorption in all its variations and also plasma emission technique. For the preparation of the samples we use a microwave digestion technique in a close container under high pressure. The spectrometers are equipped with automatic samplers and have the ability of automatic preparation of standards, automatic dilution of samples with high concetrations and automatic application of the technique of standard addition in samples with difficult substrate.

Some of our basic instruments are :

Atomic Absorption System VARIAN FS280 with 

 
Air - acetylene flame

Nitrous oxide - acetylene flame

Hydride / Vapour Generation (VGA, CV

automatic sampler SPS and

automatic diluter SIPS.

 
 




Atomic Absorption System  VARIAN AA240Z with

 
electrothermal graphite tube atomizers using Zeeman
and deuterium background correction

automatic sampler/diluter PS120



 









ICP-OES ULTIMA 2 / JOBIN YVON










 
Microwave digestion system MILLESTONE with 15 positions  


The WET CHEMISTRY LABORATORY performs all the analysis which require distillations, excractions, submersions, measurements with photometer and analysis of classical chemistry in general. Special care has been given to the optimazation of automation. The basic equipment includes:
 
Kjeldahl automatic distillation unit

Soxtec automatic extraction unit

UV-VIS  Molecular absorption spectrophotometers

FT-IR  spectrophotometers for analysis in oenological and dairy products

Isoelectric electrophoresis Focusing unit (IEF)

Vertical Slab Gel electrophoresis unit (PAGE)

The MICROBIOLOGICAL LABORATORY  occupies an entire floor and it is designed for "one-way" flow of samples, from the "cleaner" towards the most "contaminated" sections, in order to avoid contamination. There are separate premises for the preparation and sterilisation of substrates, the storage of samples. The basic equipment includes :


Laminar Flow Cabinet Class ΙΙ

Autoclave Raypa 75 lt 

VIDAS

 Stomacher device

 Sartorius multiple filtration unit

Colony counter and

Incubators
 
The ORGANOLEPTIC TEST LABORATORY operates in a special and separate space where our trained panel of testers organoleptically evaluates food and wine samples using triangle test, duo-trio test, ranking test.